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- W2080946871 abstract "The synthesis of 13C-enriched pyrrole, labeled adjacent to the nitrogen atom, is described. A convenient and effective bench-top synthesis is given which uses a readily available enriched pyranose sugar, 2-13C d-galactose, as the starting material. In the first step of the synthesis, d-galactose is oxidized to produce mucic acid in 70–75% yield. Mucic acid is then treated with ammonium hydroxide to give ammonium mucate in 99% yield. In the final step, ammonium mucate is pyrolyzed to form pyrrole with a 35% yield. The pyrrole obtained in this manner is greater than 98% enriched at the α position. Copyright © 1999 John Wiley & Sons, Ltd." @default.
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- W2080946871 date "1999-10-01" @default.
- W2080946871 modified "2023-09-27" @default.
- W2080946871 title "Synthesis of13C-enriched pyrrole from 2-13Cd-galactose" @default.
- W2080946871 doi "https://doi.org/10.1002/(sici)1099-1344(199910)42:10<927::aid-jlcr249>3.0.co;2-j" @default.
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