Matches in SemOpenAlex for { <https://semopenalex.org/work/W2080973612> ?p ?o ?g. }
Showing items 1 to 76 of
76
with 100 items per page.
- W2080973612 endingPage "662" @default.
- W2080973612 startingPage "659" @default.
- W2080973612 abstract "The INEPT experiment which uses selective 1H pulses (INAPT) was used to assign quaternary carbon NMR signals in trisubstituted alkenes. Given that 3J(CH) across the double bond is usually larger for the trans than the cis disposed nuclei, experimental conditions may be chosen such that more polarization transfer is effected in the case of the trans nuclei. We applied this approach to two important pharmaceutica Is, cyclobenzaprine and ami-triptyline, and some structurally related compounds. In each case the INAPT experiment quickly afforded a stereochemical assignment. Assignments were corroborated with the data from two-dimensional selective hetero-nuclear J-resolved and heteronuclear nuclear Overhauser effect experiments." @default.
- W2080973612 created "2016-06-24" @default.
- W2080973612 creator A5002023162 @default.
- W2080973612 date "1989-07-01" @default.
- W2080973612 modified "2023-09-27" @default.
- W2080973612 title "Utilization of the selective pulse INEPT NMR experiment (INAPT) for the facile distinction of quaternary carbons attached to a trisubstituted alkene" @default.
- W2080973612 cites W1974428156 @default.
- W2080973612 cites W1979076621 @default.
- W2080973612 cites W1992668954 @default.
- W2080973612 cites W2007486615 @default.
- W2080973612 cites W2008252896 @default.
- W2080973612 cites W2009274562 @default.
- W2080973612 cites W2028807792 @default.
- W2080973612 cites W2041104846 @default.
- W2080973612 cites W2045483551 @default.
- W2080973612 cites W2055633049 @default.
- W2080973612 cites W2060681397 @default.
- W2080973612 cites W2075079546 @default.
- W2080973612 cites W2086780808 @default.
- W2080973612 cites W2952485866 @default.
- W2080973612 doi "https://doi.org/10.1002/mrc.1260270710" @default.
- W2080973612 hasPublicationYear "1989" @default.
- W2080973612 type Work @default.
- W2080973612 sameAs 2080973612 @default.
- W2080973612 citedByCount "4" @default.
- W2080973612 crossrefType "journal-article" @default.
- W2080973612 hasAuthorship W2080973612A5002023162 @default.
- W2080973612 hasConcept C119851462 @default.
- W2080973612 hasConcept C121332964 @default.
- W2080973612 hasConcept C147597530 @default.
- W2080973612 hasConcept C147789679 @default.
- W2080973612 hasConcept C161790260 @default.
- W2080973612 hasConcept C178790620 @default.
- W2080973612 hasConcept C182155053 @default.
- W2080973612 hasConcept C185592680 @default.
- W2080973612 hasConcept C205049153 @default.
- W2080973612 hasConcept C2776254738 @default.
- W2080973612 hasConcept C46141821 @default.
- W2080973612 hasConcept C66974803 @default.
- W2080973612 hasConcept C71240020 @default.
- W2080973612 hasConcept C92381491 @default.
- W2080973612 hasConceptScore W2080973612C119851462 @default.
- W2080973612 hasConceptScore W2080973612C121332964 @default.
- W2080973612 hasConceptScore W2080973612C147597530 @default.
- W2080973612 hasConceptScore W2080973612C147789679 @default.
- W2080973612 hasConceptScore W2080973612C161790260 @default.
- W2080973612 hasConceptScore W2080973612C178790620 @default.
- W2080973612 hasConceptScore W2080973612C182155053 @default.
- W2080973612 hasConceptScore W2080973612C185592680 @default.
- W2080973612 hasConceptScore W2080973612C205049153 @default.
- W2080973612 hasConceptScore W2080973612C2776254738 @default.
- W2080973612 hasConceptScore W2080973612C46141821 @default.
- W2080973612 hasConceptScore W2080973612C66974803 @default.
- W2080973612 hasConceptScore W2080973612C71240020 @default.
- W2080973612 hasConceptScore W2080973612C92381491 @default.
- W2080973612 hasIssue "7" @default.
- W2080973612 hasLocation W20809736121 @default.
- W2080973612 hasOpenAccess W2080973612 @default.
- W2080973612 hasPrimaryLocation W20809736121 @default.
- W2080973612 hasRelatedWork W2007585072 @default.
- W2080973612 hasRelatedWork W2009105657 @default.
- W2080973612 hasRelatedWork W2058773188 @default.
- W2080973612 hasRelatedWork W2064521144 @default.
- W2080973612 hasRelatedWork W2080973612 @default.
- W2080973612 hasRelatedWork W2086862822 @default.
- W2080973612 hasRelatedWork W2095130542 @default.
- W2080973612 hasRelatedWork W2106445386 @default.
- W2080973612 hasRelatedWork W229018306 @default.
- W2080973612 hasRelatedWork W2980733414 @default.
- W2080973612 hasVolume "27" @default.
- W2080973612 isParatext "false" @default.
- W2080973612 isRetracted "false" @default.
- W2080973612 magId "2080973612" @default.
- W2080973612 workType "article" @default.