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• W2081042694 abstract "Abstract An efficient de novo synthesis of uronic acid building blocks is described. The synthetic strategy relies on the stereoselective elongation of thioacetal protected dialdehydes 12 a and 17 . The dialdehydes are prepared from D ‐xylose, a cheap and commercially available source. A highly stereoselective MgBr 2 ⋅ OEt 2 ‐mediated Mukaiyama aldol addition to C4‐aldehyde 12 a is performed to obtain D ‐glucuronic acid building block 16 , whereas L ‐iduronic acid building block 22 is prepared by MgBr 2 ⋅ OEt 2 ‐mediated cyanation of C5‐aldehyde 17 . Synthesis of a heparin disaccharide demonstrates the utility of the de novo strategy for the assembly of glycosaminoglycan oligosaccharides." @default.
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• W2081042694 date "2007-05-15" @default.
• W2081042694 modified "2023-10-18" @default.
• W2081042694 title "De Novo Synthesis of Uronic Acid Building Blocks for Assembly of Heparin Oligosaccharides" @default.
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• W2081042694 doi "https://doi.org/10.1002/chem.200700141" @default.
• W2081042694 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17444537" @default.
• W2081042694 hasPublicationYear "2007" @default.
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