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- W2081168907 abstract "Abstract New derivatization methods using chiral ferrocene reagents have been developed for the optical resolution of carboxylic acids by high-performance liquid chromatography with electrochemical detection. Two chiral derivatization reagents, 1-ferrocenylethylamine and 1-ferrocenylpropylamine, were readily prepared from acetylferrocene and propionylferrocene in two steps, respectively. Condensation of carboxylic acids with the chiral reagent was effected in the presence of water-soluble carbodiimide and 1-hydroxybenzotriazole. The diastereomeric amides formed from N-acetylamino acid and α-arylpropionic acid enantiomers were efficiently resolved by reversed-phase chromatography and showed the satisfactory sensitivity at +0.45 V vs. an Ag/AgCl reference electrode with a detection limit of 0.5 pmole (S/N=5)." @default.
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- W2081168907 date "1987-10-01" @default.
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- W2081168907 title "Ferrocene Derivatization Reagents for Optical Resolution of Carboxylic Acids by High-performance Liquid Chromatography with Electrochemical Detection" @default.
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- W2081168907 doi "https://doi.org/10.1080/01483918708068304" @default.
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