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- W2081547501 abstract "Three new monomers of p-phenylacrylamide derivatives were prepared by either the reaction of p-methyl-, p-nitro-, and p-chloroaniline with acryloyl chloride or with acrylic acid in the presence of dicyclohexyl carbodiimide (DCCI). The prepared monomers were copolymerized with each of tri-n-butyltinacrylate and tri-n-butyltinmethacrylate. Copolymerization reactions were carried out in dioxane at 70°C using 1 mol % azobisisobutyronitrile as a free radical initiator. The structure of the new monomers and the prepared copolymers were investigated by IR and 1H-NMR spectroscopy. The monomer reactivity ratios for the copolymerization of p-chlorophenylacrylamide (M1) with each of tri-n-butyltinacrylate (TBTA) and tri-n-butyltinmethacrylate (TBTMA) (M2) were found to be r1 = 2.6; r2 = 0.83 and r1 = 1.3; r2 = 1.71, respectively. In case of p-tolyacrylamide (M1) with TBTA and TBTMA (M2) r1 = 0.35, r2 = 1.03 and r1 = 1.38, r2 = 0.366 respectively. The Q and e values for the prepared p-tolyl- and p-chlorophenylacrylamide were calculated © 1993 John Wiley & Sons, Inc." @default.
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- W2081547501 date "1993-02-01" @default.
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- W2081547501 title "Effect of substitution on the reactivity of some new p-phenylacrylamide derivatives with organotin monomers" @default.
- W2081547501 doi "https://doi.org/10.1002/pola.1993.080310214" @default.
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