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- W2081551808 abstract "A high-yield synthetic route towards methyl 4″-O-methyl-β-D-cellotrioside (17) via cellobioside acceptor 8 and glucosyl fluoride donor 15 was established. The former was synthesized from cellobiose peracetate in 7 steps and 21% overall yield, while the latter was obtained from methyl β-D-glucopyranoside in a 6-step-synthesis with 19% yield. Glycosidation afforded 13% of α-compound besides the desired β-isomer (31%). The target compound, being the higher homologue of the recently prepared 4′-O-methyl-β-D-cellobioside (1), is required to study by solid-state techniques the hydrogen bond network in cellodextrins and cellulose, and its changes upon swelling and dissolution." @default.
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- W2081551808 date "2005-12-01" @default.
- W2081551808 modified "2023-09-27" @default.
- W2081551808 title "Synthesis of the Cellulose Model Compound Methyl 4″-O-Methyl-β-D-Cellotrioside" @default.
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- W2081551808 doi "https://doi.org/10.1002/masy.200551408" @default.
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