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- W2081567698 abstract "Abstract Low temperature photolysis of a hexane solution of [Ru3(CO)12] and FcC CC CFc provides a convenient route to the diyne-bridged cluster [Ru3(CO)10{μ3-FcC2C CFc}] (1). When a toluene solution containing 1 and diferrocenyldiacetylene was heated at 80 °C three compounds formed: the ruthenacyclopentadiene complex [Ru2(CO)6{C4Fc2(C CFc)2}2] (2), and two isomers of the diruthenacycloheptadienone complex, [Ru2(CO)6[μ-η1:η1:η2:η2-{FcC CCC(Fc)–C(O)–C(Fc)CC CFc}] (3), [Ru2(CO)6[μ-η1:η1:η2:η2-{FcC CCC(Fc)–C(O)–C(–C CFc)C(Fc)}] (4). Compounds 2–4 have been characterized spectroscopically and their structures established crystallographically. Consistent with structural reports on metallacyclic compounds bearing bulky substituents, in 2 and 3, the bulkier of the two types of substituents, the C CFc groups are located on the carbon atoms adjacent to the metal atoms, whereas in compound 4, only one of the two C CFc groups is on the α-carbon atom of the ruthenacyclopentadienone ring." @default.
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- W2081567698 date "2008-05-01" @default.
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- W2081567698 title "Coupling reaction between the uncoordinated acetylenic bond of [Ru3(CO)10{μ3-FcC2CCFc}] and FcCCCCFc to form [Ru2(CO)6{C4Fc2(CCFc)2}2], [Ru2(CO)6[μ-η1:η1:η2:η2-{FcCCCC(Fc)–C(O)–C(Fc)CCCFc}] and [Ru2(CO)6[μ-η1:η1: η2:η2-{FcCCCC(Fc)–C(O)–C(–CCFc)C(Fc)}]" @default.
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- W2081567698 doi "https://doi.org/10.1016/j.jorganchem.2008.02.021" @default.
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