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- W2081871211 abstract "The species [Ph3PCH2CH2PPh2+3][Ru10(μ6-C)2(CO)20(μ-CO)2-4] · 2Me2CO crystallizes in the centrosymmetric triclinic space group P1 (No. 2) with a 12.8846(25), b 15.3253(26), c 20.4478(41) Å, α 104.494(15)°, β 96.514(16)°, γ 94.674(15)°, V 3858.5(13) Å3 and Z = 2. Diffraction data (Mo-Kα, 2θ = 4.5–40.0°) were collected on a Synthex P21 diffractometer and the structure was refined to R 4.6% for those 6381 independent reflections with |Fo| > 1.0σ(|Fo|). The decanuclear dianion is based upon an edge-bridged bisoctahedron (with each octahedral fragment containing a μ6-C atom) and has approximate D2 symmetry. Each ruthenium atom is associated with two terminal carbonyl ligands; in addition, all but the edge-fused ruthenium atoms are linked pair-wise by single, symmetrically bridging carbonyl ligands. The species [NEt+4]2[Ru10(μ6-C)2(CO)20(μ-CO)2-4] has also been studied. The Ru10 cluster lies on a site of 1 symmetry (space group P21/c, Z = 2) and the resulting disorder led to only a partial solution to this structure." @default.
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- W2081871211 date "1990-09-01" @default.
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- W2081871211 title "Crystal structure of [Ph3PCH2CH2PPh2+3][Ru10(μ6-C)2(CO)20(μ-CO)2-4] · 2Me2CO and some brief comments on the severely disordered structure of [NEt+4]2[Ru10(μ6-C)2(CO)20(μ-CO)2-4]" @default.
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- W2081871211 doi "https://doi.org/10.1016/0022-328x(90)85264-y" @default.
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