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• W2081889628 abstract "Abstract Orthorhombic LiMn 1– x Al x O 2 nanocrystals ( P mmn (59), origin choice 2) with different morphologies were successfully synthesized using Mn 2 O 3 and Al 2 O 3 as Mn- and Al-sources in a 3.5 M LiOH aqueous solution hydrothermally treated at 150 °C. Although Al 3+ ions introduced into the starting hydrothermal solution was in a large amount from 0 to 0.33 of Al/Mn molar ratio, noted as Al/Mn(HT) where HT refers to hydrothermal treatment; the ratio was as low as 0.05 in the phase-pure LiMn 1– x Al x O 2 crystals, noted as Al/Mn(SS) where SS refers to solid solution, while a Al/Mn(HT) ratio higher than 0.5 resulted in the formation of orthorhombic LiAlO 2 phase. With an increase of Al/Mn(SS), the average oxidation number was higher than 3 and gradually increased, leading to a monotonous shrinkage of the unit cell along a -axis (the zigzag direction of the metal-oxygen octahedron layers). Furthermore, Al 3+ also influenced on the morphology of the crystals: (1) cuboid shaped crystals as (Al/Mn(SS)   0.02 can be obtained. Galvanostatic measurement exhibited that the capacity of the electrode composed of Li 0.93 Mn 0.96 Al 0.04 O 2 can reach a discharge capacity of 175 mAh/g at a current density of 0.1 C and the capacity retention could be 82.9% after 25th cycling, showing that Al 3+ can stabilize the layered structure by retarding its transforming to spinel one." @default.
• W2081889628 created "2016-06-24" @default.
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• W2081889628 date "2013-08-01" @default.
• W2081889628 modified "2023-09-26" @default.
• W2081889628 title "Influence of Al3+ ions on the morphology and structure of layered LiMn1–xAlxO2 cathode materials for the lithium ion battery" @default.
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• W2081889628 doi "https://doi.org/10.1016/j.jallcom.2013.03.187" @default.
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