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• W2082023346 abstract "Chemical insertion of Li in NbO2F has been performed under various conditions. NbO2F prepared from Nb-metal and a mixture of HF(aq) and HNO3(aq) was used as starting material, since NbO2F made from Nb2O5 and HF(aq) was shown to be NbO2F · HF. The products, with the formula LixNbO2F (0 < x ≤ 1.8), have been analyzed for Li content using atomic absorption spectrometry. According to the X-ray powder diffraction results, the Li-incorporated samples with 0.2 < x < 1.3 contained two phases, namely, one of cubic and one of hexagonal symmetry, whereas specimens with x > 1.3 were single phase of a hexagonal structure type. Samples with x = 0.0, 0.3, 0.5, and 1.2 were studied by electron diffraction and high-resolution electron microscopy techniques. Crystals of specimen x = 0.3 were shown to consist predominantly of a cubic phase surrounded by a shell of hexagonal LiNbO3 structure type, while the crystals of Li1.2NbO2F seemed to be built up mainly of the hexagonal phase." @default.
• W2082023346 created "2016-06-24" @default.
• W2082023346 creator A5017134006 @default.
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• W2082023346 date "1989-07-01" @default.
• W2082023346 modified "2023-10-16" @default.
• W2082023346 title "Li-inserted NbO2F studied by high-resolution electron microscopy and X-ray powder diffraction" @default.
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• W2082023346 doi "https://doi.org/10.1016/0022-4596(89)90196-5" @default.
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