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• W2082081434 abstract "Ionic conducting glasses in thin film forms are promising candidates for applications in microelectronics devices such as microbatteries and microsupercapacitors. In recent years, it was shown that physicochemical properties of thin films may differ substantially from those of the target bulk materials. Thus, it remains a challenge in science and thin film technology to control the properties of thin films in terms of chemical composition and conditions of manufacturing. This work presents a structural investigation of lithium−borate thin film electrolytes prepared by rf sputtering of Li−diborate targets. Chemically stable thin films ca. 1 μm thick were deposited on Si and gold-covered Si substrates under argon and their infrared spectra were measured in a broad spectral range (30−5000 cm-1). The spectra of thin films were modeled on the basis of rigorous expressions for reflectance and transmittance of the film/substrate bilayer system. The experimental results for thin films were compared with those simulated by using the optical response functions of bulk glasses xLi2O−(1−x)B2O3 (x = 0.33, 0.30, 0.275, 0.25), which were prepared by the conventional melt quenching technique. The comparison of experimental and simulated spectra showed that rf sputtering of Li−diborate targets (x = 0.33) leads to Li−borate thin films with lithium oxide content lower than that of the target material. Best agreement between experimental and simulated thin film spectra was obtained for x = 0.275, after proper annealing of thin films to remove differences in thermal history between thin film and bulk glass states." @default.
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• W2082081434 date "2007-05-16" @default.
• W2082081434 modified "2023-09-24" @default.
• W2082081434 title "Thin Film Amorphous Electrolytes: Structure and Composition by Experimental and Simulated Infrared Spectra" @default.
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• W2082081434 doi "https://doi.org/10.1021/jp068617b" @default.
• W2082081434 hasPublicationYear "2007" @default.
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