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• W2082173700 startingPage "727" @default.
• W2082173700 abstract "Abstract The functionalized triaryl phosphine tris(2,4,6-trimethoxyphenyl)phosphine (TMPP) was prepared and characterized by single crystal X-ray diffraction studies and multinuclear NMR spectroscopy. The asymmetric unit contains two independent molecules of TMPP on general positions that adopt a pseudo-propeller arrangement of the arene substituents. The basicity of TMPP was evaluated by measuring the νA1(CO) stretching mode for the complex Ni(CO)3L; the value for Ni(CO)3TMPP is νA1(CO) = 2048 cm−1, which is the lowest reported value for a tertiary phosphine complex (PR3)Ni(CO)3. The phosphine oxide derivative, tris(2,4,6-trimethoxyphenyl)phosphine (TMPPO), was prepared by oxidation with H2O in refluxing acetone. In the structure of TMPPO, the oxygen atom of the phosphine oxide is hydrogen bonded to two interstitial water molecules. Both the phosphine and phosphine oxide compounds were fully characterized by a variety of physical and spectroscopic techniques, including NMR (1H, 31P, 13C), IR and electronic absorption spectroscopies and cyclic voltammetry." @default.
• W2082173700 created "2016-06-24" @default.
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• W2082173700 date "1994-01-01" @default.
• W2082173700 modified "2023-09-25" @default.
• W2082173700 title "Synthesis and properties of tris(2,4,6-trimethoxyphenyl)phosphine and tris(2,4,6-trimethoxyphenyl)phosphine oxide" @default.
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• W2082173700 doi "https://doi.org/10.1016/s0277-5387(00)81676-9" @default.
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