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- W2082220281 abstract "Two samples of rod-like micelles in decane were prepared by seeded growth from a sample of a poly(isoprene-b-ferrocenyldimethylsilane) diblock copolymer (PI1000–PFS50, where the subscripts indicate the degree of polymerization). These micelles were uniform in length with a mass/length of 1.9 molecules/nm. The longer micelles (L-1250) had a number-average length Ln = 1243 nm, whereas the shorter micelles (L-250) had Ln = 256 nm. We used transmission electron microscopy (TEM) to examine the behavior of these micelles when dilute solutions of L-1250 or L-250 or their mixtures were heated at temperatures ranging from 40 to 75 °C and then cooled to room temperature. At 55 °C, the L-1250 sample underwent kinetically controlled fragmentation to give a broad distribution of micelle lengths. At this temperature, fragmentation was much less prominent in the L-250 sample. At higher temperatures, micelles with narrow distributions of lengths were obtained in each case (Lw/Ln ≈ 1.01). This process operates under therm..." @default.
- W2082220281 created "2016-06-24" @default.
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- W2082220281 date "2012-10-10" @default.
- W2082220281 modified "2023-10-17" @default.
- W2082220281 title "Polyferrocenylsilane Crystals in Nanoconfinement: Fragmentation, Dissolution, and Regrowth of Cylindrical Block Copolymer Micelles with a Crystalline Core" @default.
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- W2082220281 doi "https://doi.org/10.1021/ma3014788" @default.
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