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• W2082285467 abstract "An effective method was developed for screening licorice roots and fritillary bulbs for contamination by aflatoxin B1 and ochratoxin A using high-performance liquid chromatography connected to tandem mass spectrometry (HPLC–MS/MS). The samples were pre-concentrated and purified using solid-phase extraction, which provided satisfactory results. The separation was performed on a Waters XbridgeTM C18 column with a linear gradient of acetonitrile - water containing 5 mM ammonium acetate. The MS spectrum was acquired in positive mode with both single quadrupole (Q1) and multiple reaction monitoring (MRM). The optimised method offered a good linear correlation (r2 > 0.9967), excellent precision (RSD < 2.83%) and acceptable recovery (from 92.78 to 105.37%). The limits of detection (LOD) and the limits of quantification (LOQ) were less than 0.024 μg/kg and 0.095 μg/kg, respectively. The validated method was successfully applied to the rapid screening for AFB1 and OTA in licorice roots and fritillary bulbs." @default.
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• W2082285467 date "2013-06-01" @default.
• W2082285467 modified "2023-10-17" @default.
• W2082285467 title "Simultaneous determination of aflatoxin B1 and ochratoxin A in licorice roots and fritillary bulbs by solid-phase extraction coupled with high-performance liquid chromatography–tandem mass spectrometry" @default.
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• W2082285467 doi "https://doi.org/10.1016/j.foodchem.2012.11.066" @default.
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