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- W2082568562 abstract "Synthesis and pyrolysis of a soluble precursor possessing an Nb-N backbone structure were investigated. The precursor was prepared by aminolysis reaction of tetrakis(diethylamido)niobium with isopropylamine. The precursor was soluble in benzene, and had a polymeric structure possessing Nb-N-Nb imido-bridges. The precursor was pyrolyzed under NH3-N2 (at 600 °C for 2 h under NH3 and subsequently at 1350 °C for 8 h under N2) and Ar (at 1500 °C for 2 h) atmospheres. δ-NbN was obtained as a main crystalline phase after the pyrolysis of the precursor under NH3-N2, whereas pyrolysis of the precursor under Ar led to the formation of NbC as the only crystalline phase. More than 90% of niobium which was present in the precursor remained in both of the pyrolyzed products." @default.
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- W2082568562 date "2000-05-01" @default.
- W2082568562 modified "2023-10-03" @default.
- W2082568562 title "Synthesis of a Soluble Precursor Possessing an Nb-N Backbone Structure and Its Pyrolytic Conversion into Niobium-Based Ceramics" @default.
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- W2082568562 doi "https://doi.org/10.1246/bcsj.73.1299" @default.
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