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• W2082783120 abstract "[Pt(COD)Cl2] (1) reacts with PPh2(C6H4COOH) (2a,b,c), PPh2(C6H4COONa) (2d), PPh(C6H4COOH)2 (4b,c) and P(C6H4COOH)3 (6b,c) with formation of the corresponding complexes [Pt(L)2Cl2] (3a,b,c,d, 5b,c, 7b,c). Halide abstraction from 3a by Ag+ promotes coordination of the ortho-carboxylate function to platinum, yielding [Pt{PPh2(C6H4COO-2)}{PPh2(C6H4COOH-2)}Cl] (bd8) and [ovbar|{PPh2(C6H4COO-2)}2] (bd9). Reaction of 1 with CO and 2a or 2b gives [Pt(CO)(L)Cl2] (10a,b), wherea 1 and 2,3-bis(diphenylphosphino) maleic anhydride yields [PtPh2PC=C(PPh2)COOOCO}Cl2] (bd12) and [Pt{Ph2PC(COOH)=C(COOMe)-PPh2}Cl2] (13). The 1H, 13C and 31P NMR spectra are reported and discussed. The X-ray structural analysis of 3b showed the compound to be monoclinic, space group P21/n, Z=4, with a=1038.5(3), b=1792.6(4), c=2311.5(4) pm, β=91.6(2)° and Dcalc=1.353 g cm−3. The structure was solved from 4832 observed reflections with F0 > 4 σ(F0) and refined to a final R value of 0.0743. The Pt atom is surrounded by two Cl and two P atoms in a square planar arrangement." @default.
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• W2082783120 date "1995-12-01" @default.
• W2082783120 modified "2023-10-14" @default.
• W2082783120 title "Synthesis and structure determination of some platinum (II) complexes with hydrophilic carboxylated tertiary phosphine ligands" @default.
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• W2082783120 doi "https://doi.org/10.1016/0020-1693(95)04528-7" @default.
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