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- W2082933671 abstract "Treatment of the di-μ-chloride allyl palladium complex [(η3-C4H7)Pd(μ-Cl)2Pd(η3-C4H7)] with [NBu4]OH (1:2 molar ratio) in methanol, followed by addition of phenol or para-substituted phenol ArOH (1:2 molar ratio), allows the preparation of dimeric aryloxo complexes of the type [(η3-C4H7)Pd(μ-OAr)2Pd(η3-C4H7)] (Ar=Ph 1, C6H4Me-p 2, C6H4Cl-p 3, C6H4Br-p 4). The addition of p-nitrophenol or pentafluorophenol to complex 1 results in quantitative substitution of the phenoxide anion to give the di-μ-aryloxo palladium complexes [(η3-C4H7)Pd(μ -OAr)2Pd(η3-C4H7)] (Ar=C6H4NO2-p 5 or C6F5 6). Complexes 1, 5 and 6 react with PPh3 to give the monomeric aryloxo complexes [(η3-C4H7)Pd(OAr)(PPh3)] (Ar=Ph 7, C6H4NO2-p 8, C6F5 9). The identity of these complexes has been established by partial elemental analyses and NMR (1H, 19F, 13C and 31P) spectroscopy." @default.
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- W2082933671 date "1999-07-01" @default.
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- W2082933671 title "New aryloxo allylpalladium complexes" @default.
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- W2082933671 doi "https://doi.org/10.1016/s0277-5387(99)00105-9" @default.
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