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• W2082998652 abstract "Hecogenin acetate 5 was converted to an intermediate suitable for the construction of a C14',15' dihydro derivative of the “South” hexacyclic spiroketal of cephalostatin 1 1. The key transformations include: (i) proximal functionalization of the C-18 methyl group in 17 via hypoiodite homolysis; (ii) Rhodium [II] catalyzed intermolecular oxygen alkylation of primary neopentyl hydroxyl group in 20 and (iii) intramolecular Wadsworth-Emmons reaction to provide 23, the ester precursor of aldehyde 4" @default.
• W2082998652 created "2016-06-24" @default.
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• W2082998652 date "1995-11-01" @default.
• W2082998652 modified "2023-10-16" @default.
• W2082998652 title "Synthesis of a C14',15' dihydro derivative of the south hexacyclic steroid unit of cephalostatin 1. Part I : regiospecific Rh[II]-mediated intermolecular oxygen alkylation of a primary neopentyl alcohol" @default.
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• W2082998652 doi "https://doi.org/10.1016/0040-4039(95)01804-q" @default.
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