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• W2083093028 abstract "Treatment of ascomycin or its O-TBDMS-derivatives with hydrogen sulfide and pyridine in dimethylformamide solution results in deoxygenation reactions at the tricarbonyl sequence of the binding domain. 9-deoxo-ascomycins (5a-c) are obtained in high yields (75–85%) together with small amounts (2–14% yield) of 10-deoxo-ascomycins (6a-c). The novel derivative 10-deoxo-ascomycin (6a) is accessible in excellent yield (85%) from the 10-amino-analog of ascomycin upon reaction with hydrogen sulfide in the absence of base." @default.
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• W2083093028 date "1999-10-01" @default.
• W2083093028 modified "2023-10-17" @default.
• W2083093028 title "Carbonyl to methylene conversions at the tricarbonyl-portion of ascomycin derivatives" @default.
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• W2083093028 doi "https://doi.org/10.1016/s0040-4039(99)01622-6" @default.
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