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- W2083103432 abstract "The on-line coupling of a small digital computer to a liquid chromatograph is described. A new real-time language, MIRACL II, is used for programming. The experimental set-up is presented and a ndw automatic sample loop valve is described. The system has been studied in terms of the precision in peak area, peak height and retention attainable with commercial liquid chromatographic equipment. Precision in peak area and height is found to be significantly improved with the sampling valve relative to syringe injection. The influence of several pumping systems on precision was also studied and marked differences in the relative standard deviations of peak area and height were found. The relationship of the relative standard deviation of the peak area to sample size has also been studied. In addition, the important role of the flow-rate of the mobile phase on detection limits and precision is shown. Finally, some results are presented on the reproducibility of retention over short and long time periods." @default.
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- W2083103432 date "1973-08-01" @default.
- W2083103432 modified "2023-10-11" @default.
- W2083103432 title "A study of precision in modern liquid Chromatography using a dedicated computer" @default.
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- W2083103432 doi "https://doi.org/10.1016/s0021-9673(00)97046-8" @default.
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