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- W2083111135 abstract "(1) Chlorination of DL-N-benzoylallothreonine ethyl ester with thionyl chlodide in benzene in the presence of pyridine gave the lower-melting isomer of ethyl-DL-α-benzamido-β-chlorobutyrate, m. p. 84.5-86.5°, in a yield of 57%. On the other hand, chlorination with phosphorus pentachloride in chloroform gave the higher-melting isomer, m. p. 99-100°. (2) Two isomers of α-benzamido-β-benzylmercaptobutyric acid (derivatives of thiothreonine A and B) were synthesised. The chlorine atom of ethyl DL-α-benzamido-β-chlorobutyrate could be replaced by a sulfhydryl group by the action of benzyl mercaptan. A remarkable effect of different solvents on this replacement reaction was described." @default.
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- W2083111135 date "1951-05-01" @default.
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- W2083111135 title "Synthetic Studies on Thiothreonines. II" @default.
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- W2083111135 doi "https://doi.org/10.1246/bcsj.24.239" @default.
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