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• W2083114733 endingPage "1559" @default.
• W2083114733 startingPage "1553" @default.
• W2083114733 abstract "Up to eight redox-active ferrocenyl units have been incorporated, through the unsaturated ethynyl linkers, on the periphery of a series of cyclic tetrapyrrole derivatives including zinc(II) phthalocyanine and 2,3-naphthalocyanine, and nickel(II) meso-diphenylporphyrin. The synthesis of the former two macrocycles 4 and 7 involves the Sonogashira coupling reaction of ferrocenylethyne with 4,5-dichlorophthalonitrile (1) or 6,7-dibromonaphthalonitrile (5), respectively, followed by a base-promoted cyclization. The meso-bis(ferrocenylethynyl)porphyrin 11 has been prepared from the dibromo analogue 10 also by a palladium-catalyzed coupling reaction. These novel macrocyclic compounds have been spectroscopically and electrochemically characterized. As revealed by cyclic voltammetry, the ferrocenyl moieties appear to be electrochemically independent in these complexes and there is no significant electronic coupling among the iron(II) centers." @default.
• W2083114733 created "2016-06-24" @default.
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• W2083114733 date "2001-02-06" @default.
• W2083114733 modified "2023-10-03" @default.
• W2083114733 title "Tetrapyrrole Derivatives Substituted with Ferrocenylethynyl Moieties. Synthesis and Electrochemical Studies" @default.
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• W2083114733 doi "https://doi.org/10.1021/jo0004308" @default.
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