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• W2083130704 abstract "A facile route for the synthesis and isolation of 1,2,3,12b-tetrahydroimidazo[1,2-f]phenanthridines (TIPs) has been developed. The heterocycle is a reactive intermediate in the three-step cascade synthesis of 2,3-dihydro-1H-imidazo[1,2-f]phenanthridinium cations (DIPs), a biologically active DNA intercalating framework; however, the intermediate has previously only been characterized in situ. Derivatization of the structure at the imidazo-N position controls the reactivity of the intermediate with respect to electronic potential and pKa allowing isolation of a selection of TIP structures. Correlations between these parameters and reaction outcome have been made, and other influences such as steric and solvent effects have also been investigated." @default.
• W2083130704 created "2016-06-24" @default.
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• W2083130704 date "2009-10-06" @default.
• W2083130704 modified "2023-09-23" @default.
• W2083130704 title "Fine Tuning Reactivity: Synthesis and Isolation of 1,2,3,12b-Tetrahydroimidazo[1,2-<i>f</i>]phenanthridines" @default.
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• W2083130704 doi "https://doi.org/10.1021/jo901622e" @default.
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