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• W2083173683 startingPage "3269" @default.
• W2083173683 abstract "We have extended the methodology developed for the preparation of atropisomeric chiral ligands derived from the MeOBIPHEP ligand to water-soluble ones. The hydrophilic ligands bearing sodium carboxylate and methylammonium chloride moieties were easily synthesized under mild conditions in a short sequence and in high yields. Their solubility and acid/base properties were also determined. The ruthenium(II) catalysts contain- ing 4-CO2Na- and 3,5-(CO2Na)2-substituted MeOBIPHEP analogues showed excellent activities and led to the desired hydrogenated products derived from dimethyl itaconate and 2-(4-fluorophenyl)-3-methylcrotonic acid in ees≥92%. An investigation of the asymmetric hydrogenation of the latter substrate in D2O as solvent afforded an insight into the mechanism." @default.
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• W2083173683 date "2011-11-29" @default.
• W2083173683 modified "2023-10-16" @default.
• W2083173683 title "Synthesis of New Water-Soluble Atropisomeric Ligands Derived from the MeOBIPHEP Skeleton: Applications for Asymmetric CH Bond Formation and Mechanistic Studies" @default.
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• W2083173683 doi "https://doi.org/10.1002/adsc.201100535" @default.
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