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- W2083348178 abstract "In the present study poly(hexamethylene 2,5-furan dicarboxylate) (PHF), a polyester prepared from monomers derived from renewable resources, was synthesized by applying the melt polycondensation method. The polymer exhibited a melting temperature of about 145 °C while the glass transition temperature was 7 °C. After isothermal crystallization, PHF showed multiple melting behavior which was attributed to partial melting–recrystallization and final melting. The equilibrium melting temperature of the polymer was found to be 157 °C, while the heat of fusion of the purely crystalline material was found to be 34 kJ/mol (143 J/g). A crystallization regime I to regime II transition was observed at 134 °C as a breakpoint in the Lauritzen–Hoffman plot. The KgI and KgII values were calculated 0.9 × 105 and 1.76 × 105 respectively. Polarized optical microscopy was also employed for the study of the isothermal crystallization of PHF. PHF can be regarded thermally stable since its decomposition starts above 350 °C. Thermal degradation kinetics were investigated by means of thermogravimetric analysis." @default.
- W2083348178 created "2016-06-24" @default.
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- W2083348178 date "2015-06-01" @default.
- W2083348178 modified "2023-10-07" @default.
- W2083348178 title "Furan-based polyesters from renewable resources: Crystallization and thermal degradation behavior of poly(hexamethylene 2,5-furan-dicarboxylate)" @default.
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- W2083348178 doi "https://doi.org/10.1016/j.eurpolymj.2014.08.031" @default.
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