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• W2083365394 abstract "A new family of associating polymers based on four-arm, star-shaped poly(d,l-lactide) (PDLLA) containing peripheral complementary hydrogen-bonding sites is described. Hydroxy-terminated, four-arm, star-shaped PDLLAs of controlled molar mass were functionalized with complementary DNA base pairs, adenine (A) and thymine (T), to obtain PDLLA−A and PDLLA−T, respectively. 1H NMR spectroscopy confirmed quantitative functionalization and the subsequent formation of PDLLA−A and PDLLA−T hydrogen-bonded complexes. Job's analysis revealed a 1:1 optimal stoichiometry for the hydrogen-bonded complexes, and the association constant (Ka) that was determined using the 1H NMR-based Benesi−Hildebrand treatment was 84 M-1 for the low molar mass complementary polymers. Furthermore, the PDLLA-based hydrogen-bonded complexes exhibited higher solution viscosities compared to the corresponding non-hydrogen-bonded precursors, which further confirmed strong complementary multiple-hydrogen-bonding associations between the star-shaped polymers with terminal adenine and thymine groups. Moreover, variable-temperature 1H NMR studies demonstrated the thermoreversibility of the hydrogen-bonded PDLLA-based complexes in solution." @default.
• W2083365394 created "2016-06-24" @default.
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• W2083365394 date "2006-12-07" @default.
• W2083365394 modified "2023-10-10" @default.
• W2083365394 title "Association of Star-Shaped Poly(<scp>d</scp>,<scp>l</scp>-lactide)s Containing Nucleobase Multiple Hydrogen Bonding" @default.
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• W2083365394 doi "https://doi.org/10.1021/bm060869v" @default.
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