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- W2083443414 abstract "The complexes [{SnCl4(L)}n]1, (SnBuCl3(L)2]2 and [{SnR2Cl2(L)}n](R = Me 3 or Ph 4)[L = cyclosarcosylsarcosine (1,4-dimethylpiperazine-2,5-dione)] have been prepared and structurally characterized in the solid state by means of 119Sn Mössbauer spectroscopy, the determination of lattice dynamics by temperature-dependent 119Sn Mössbauer spectroscopy and by vibrational studies. The structure of complex 4 has been determined by X-ray crystallography and consists of infinite zigzag polymeric chains of trans-diphenyltin(IV) bridged by ketonic oxygen atoms. Each tin(IV) atom is surrounded by two carbons [Sn–C 2.129(7), 2.146(8)Å; C–Sn–C 160.1 (3)°], two chlorides [Sn–Cl 2.450(2)Å, Cl–Sn–Cl 98.5(1)°] and two oxygen atoms [Sn–O 2.370(6), 2.468(6)Å; O–Sn–O 86.1(2)°]. Tin-119 Mössbauer and vibrational data are discussed in terms of the crystal structure and the proposed structures. From the variable-temperature Mössbauer effect, the Debye temperatures for 1–4 were determined to be 144, 102, 128 and 123 K respectively." @default.
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- W2083443414 date "1995-01-01" @default.
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- W2083443414 title "Synthesis and characterization of tin(IV) and organotin(IV) 1,4-dimethylpiperazine-2,5-dione (cyclosarcosylsarcosine) adducts" @default.
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- W2083443414 doi "https://doi.org/10.1039/dt9950000123" @default.
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