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• W2083996819 abstract "Abstract New [(Q)2CUII] and [(Q)2(L)CuII] derivatives (in general QH is 1-R-3-methyl-4R′-pyrazol-5-one; in particular: Q′H : R = C6H5, R′ = C6H5(C0) ; Q″H : R =C6H5, R′= CH3(CO) ; QFH : R = C6H5, R′ = CF3(CO) ; Q″H : R = C6H5, R′ = CCl3 (CO); QBrH : R = C6H5, R′ = p-BrC6H4(CO) ; QAH : R =C6H5, R′ = p-CH3O-C6H4 (CO), QEH : R = C6H5, R′= C6H13(C0) ; QMH : R = CH3, R′= C6H5(C0); QDH : R = CH3, R = CH3(C0) ; QBH : R = C6H5, R′ = C6H5(CN(p-CH3C6H4)); L = 2,2′-bipyridine or 1,10-phenanthroline) were synthesized and characterized through analytical and spectral techniques. When (Q)2CuII interacted with an excess of PPh3, reduction to copper(I) was observed and (Q)CuI(PPh3)2 complexes were synthesized. The complex (QF)CuI(PPh3)2 was characterized by single crystal X-ray diffraction. The coordination environment of copper is a distorted tetrahedron: the P-Cu-P angle is 127.8(1) and the ligand “bite” OCu0 angle is 87.8(3)°; the Cu0 bond distances are 2.075(7) and 2.109(7) A, while CuP are 2.246(3) and 2.254(3) A." @default.
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• W2083996819 date "1996-08-01" @default.
• W2083996819 modified "2023-09-27" @default.
• W2083996819 title "Synthesis and characterization of copper(I) and copper(II) coordination compounds containing 4-acylpyrazolon-5-ato ligands. crystal structure of [(4-trifluoroacetyl-1-phenyl-3-methylpyrazolon-5-ato)bis (triphenylphosphine)copper(I)]" @default.
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• W2083996819 doi "https://doi.org/10.1016/0277-5387(96)00104-0" @default.
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