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- W2084021070 abstract "The resolution of α-methyl-α-amino acids derivatized as either N-trifluoroacetyl (TFA) isopropyl esters or N-TFA- tert -butylamides was investigated on chiral diamide stationary phases R‴CHONHCH(R″)CONHR′, where R″ = methyl, isobutyl, phenyl, benzyl. The alanine phase (I) is the solvent which shows chiral recognition for a relatively wide range of the N-TFA isopropyl esters. On the other hand, the N-TFA- tert -butylamides, including that of isovaline, are well resolved on all phases studied. In particular, the phenylalanine phase (IV) shows high resolution factors and is recommended for enantiomeric analysis of the α-methyl-α-amino acids via their N-TFA- tert -butylamides. Similarities and differences between the behaviour of α-methyl and α-H-amino acid derivatives are discussed." @default.
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- W2084021070 date "1982-04-01" @default.
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- W2084021070 title "Resolution of α-methyl-α-amino acid derivatives by gas chromatography on optically active diamide stationary phases" @default.
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- W2084021070 doi "https://doi.org/10.1016/s0021-9673(00)82708-9" @default.
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