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- W2084328235 abstract "Abstract The cadmium(II)-substituted tungstoarsenate [Cd 4 Cl 2 ( B -α-AsW 9 O 34 ) 2 ] 12− ( 1 ) has been synthesized and characterized in the solid state by XRD, IR, elemental analysis and in solution by 183 W and 111 Cd NMR. Single crystal X-ray analysis was carried out on Cs 4 K 3 Na 5 [Cd 4 Cl 2 ( B -α-AsW 9 O 34 ) 2 ] · 20H 2 O. Polyanion 1 consists of two lacunary [ B -α-AsW 9 O 34 ] 9− Keggin moieties linked via a rhomblike (Cd 4 O 14 Cl 2 ) group leading to a sandwich-type structure. Interestingly, the two external Cd atoms have a terminal Cl ligand, but the derivative with terminal water ligands, [Cd 4 (H 2 O) 2 ( B -α-AsW 9 O 34 ) 2 ] 10− ( 2 ), can also be prepared as shown by 183 W and 111 Cd solution NMR." @default.
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- W2084328235 date "2005-05-01" @default.
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- W2084328235 title "Structure and solution properties of the cadmium(II)-substituted tungstoarsenate [Cd4Cl2(B-α-AsW9O34)2]12−" @default.
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