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• W2084375504 abstract "The principle of integral metal–organic framework (MOF) reconstruction is demonstrated for differently degraded HKUST-1 via a facile, one-step, solvent-assisted treatment. Controlled MOF degradation by exposure to 77% humidity, liquid water, and diluted hydrochloric acid produces a mixture of non-porous crystalline hybrid materials containing protonated linker and copper-oxo species, which are then reconstructed back into high-quality HKUST-1 by contacting them with ethanol. X-ray diffraction and sorption kinetics reveal a true memory effect of the system from completely degraded materials. The reconstruction approach is consequently extrapolated to gas- and liquid-phase treatments in a fixed-bed reactor with ethanol and ethanol/water mixtures for use in CO2 capture from a simulated pre-combustion gas stream. Up to a maximum of 94% porosity and 85% CO2 sorption capacity can be recovered from a steamed material. A degradation-reconstruction model is put forward based on X-ray diffraction observations and structural analyses, microscopy, N2 sorption, thermogravitry–mass spectrometry and IR spectroscopy observations, particularly elucidating the influence of various degradation pathways on the reconstruction." @default.
• W2084375504 created "2016-06-24" @default.
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• W2084375504 date "2014-02-20" @default.
• W2084375504 modified "2023-10-16" @default.
• W2084375504 title "Solvent-Mediated Reconstruction of the Metal-Organic Framework HKUST-1 (Cu₃(BTC)₂)" @default.
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• W2084375504 doi "https://doi.org/10.1002/adfm.201303678" @default.
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