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- W2084509623 abstract "Abstract In the solid state the mononuclear tetrahedral complex dibromobis(4-vinylpyridine)zinc shows a reversible crystal-to-crystal phase transition which was studied by temperature dependent single crystal X-ray diffraction experiments. At low temperatures the compound crystallizes in space group P 1̅ with one ordered complex molecule in general position. Results derived from an intensity data set collected at 120 K are reported. Above the phase transition at 207 K both the cell metric and the symmetry of the diffraction pattern allow the transformation to a centered monoclinic unit cell in space group C 2/ c . In this high temperature phase the molecule is located on a twofold crystallographic axis and shows disorder with respect to the orientation of the vinyl substituent. The crystal and molecular structure based on a data collection at 293 K is described." @default.
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- W2084509623 date "2003-11-01" @default.
- W2084509623 modified "2023-10-03" @default.
- W2084509623 title "Reversible crystal-to-crystal phase transition in dibromobis(4-vinylpyridine)zinc" @default.
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- W2084509623 doi "https://doi.org/10.1524/zkri.218.11.761.20299" @default.
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