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• W2084935419 abstract "Ethyl 2,4-dioxo-4-phenylbutyrate obtained by condensation of acetophenone with diethyl oxalate is reduced enantio- and regiospecifically by baker’s yeast in a diisopropyl ether/water two-phase system to give (−)-ethyl (R)-2-hydroxy-4-oxo-4-phenylbutyrate with an ee = 98% in 80% isolated yield. The hydroxyester was hydrogenated over Pd–C to obtain (−)-ethyl (R)-2-hydroxy-4-phenylbutyrate (HPB ester), an important intermediate for the synthesis of ACE inhibitors. Prolonged contact of the reduction product with baker’s yeast produced 3-phenyl 3-oxo propanol in 90% yield." @default.
• W2084935419 created "2016-06-24" @default.
• W2084935419 creator A5064209814 @default.
• W2084935419 creator A5076245539 @default.
• W2084935419 date "2004-11-01" @default.
• W2084935419 modified "2023-09-23" @default.
• W2084935419 title "Enantio- and regiospecific reduction of ethyl 4-phenyl-2,4-dioxobutyrate with baker’s yeast: preparation of (R)-HPB ester" @default.
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• W2084935419 doi "https://doi.org/10.1016/j.tetasy.2004.09.007" @default.
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