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• W2084948470 abstract "A pressure-assisted capillary zone electrophoresis method was developed to determine the pKa values of a triptolide derivative (LLDT-246) and its impurities. The method was performed in an uncoated fused-silica capillary under the electric voltage of 18kV and 50mbar of external pressure applied simultaneously. A series of running electrolyte buffers were used with pH ranging between 2.2 and 10.0 with the constant ionic strength of 0.05M. The values of pKa of LLDT-246 and two impurities were calculated based on the pH dependence of effective mobilities (μeff). The pKa value of LLDT-246 was in good agreement with that of determined by potentiometric titration method." @default.
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• W2084948470 date "2014-01-01" @default.
• W2084948470 modified "2023-10-16" @default.
• W2084948470 title "Determination of pKa values of a triptolide derivative and its impurities by pressure-assisted capillary electrophoresis" @default.
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• W2084948470 doi "https://doi.org/10.1016/j.jpba.2013.08.012" @default.
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• W2084948470 hasPublicationYear "2014" @default.
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