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- W2085093036 abstract "Pechini polymeric precursor method was successfully used to synthesize (Ba0.95Ca0.05)(Ti0.85Zr0.15)O3 nano powders. The results of TG/DTA, XRD and IR analyses showed that by heating the precursor between 490 °C and 580 °C, an intermediate phase with possible composition of (Ba,Ca)2(Ti,Zr)2O5CO3 was formed. Between 580 °C and 700 °C, the intermediate phase transformed to a crystalline solid solution by de-carbonation reaction. The transformation completed at 700 °C. Nano-sized powders with equivalent sphere diameters about 72 nm were obtained by calcination of the precursor at 700 °C for 4 h. The ceramics sintered at 1300 °C for 2 h can reach about 95% theoretical density and the peak dielectric constant is 15,000 at 70 °C." @default.
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- W2085093036 date "2012-01-01" @default.
- W2085093036 modified "2023-10-15" @default.
- W2085093036 title "A study on the synthesis of (Ba,Ca)(Ti,Zr)O3 nano powders using Pechini polymeric precursor method" @default.
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- W2085093036 doi "https://doi.org/10.1016/j.ceramint.2011.08.001" @default.
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