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• W2085156317 startingPage "7758" @default.
• W2085156317 abstract "We provide evidence of low-temperature hydrogen evolution and possible hydrogen trapping in an anthracite coal derivative, formed via reactive ball milling with cyclohexene. No molecular hydrogen is added to the process. Raman-active molecular hydrogen vibrations are apparent in samples at atmospheric conditions (300 K, 1 bar) for samples prepared 1 year previously and stored in ambient air. Hydrogen evolves slowly at room temperature and is accelerated upon sample heating, with a first increase in hydrogen evolution occurring at approximately 60 °C. Subsequent chemical modification leads to the observation of crystalline carbons, including nanocrystalline diamond surrounded by graphene ribbons, other sp2−sp3 transition regions, purely graphitic regions, and a previously unidentified crystalline carbon form surrounded by amorphous carbon. The combined evidence for hydrogen trapping and carbon crystallization suggests hydrogen-induced crystallization of the amorphous carbon materials, as metastable hydrogenated carbons formed via the high-energy milling process rearrange into more thermodynamically stable carbon forms and molecular hydrogen." @default.
• W2085156317 created "2016-06-24" @default.
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• W2085156317 date "2006-05-27" @default.
• W2085156317 modified "2023-10-16" @default.
• W2085156317 title "Combined Hydrogen Production and Storage with Subsequent Carbon Crystallization" @default.
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• W2085156317 doi "https://doi.org/10.1021/ja0604818" @default.
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