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- W2085211212 abstract "Three characteristic waxes, dimycocerosates of the phthiocerol family, have been detected in the free lipids and also acid methanolysates of Mycobacterium tuberculosis by use of a special two-dimensional thin-layer Chromatographic system. Reductive degradation of the least, intermediate and most polar waxes gave mycocerosic alcohols in all cases and phthiocerol A, phthiocerol B and phthiotriol A, respectively. The most polar wax was selectively reduced by sodium borohydride, showing that the diol constituent was a keto component, phthiodiolone A, rather than the reduced compound, phthiotriol A. Gas chromatography and mass spectrometry of all the wax reduction products showed that the myococerosates were the expected tri- and tetramethyl branched acids, with a C32 main component, and the phthiocerols A, B and phthiodiolone A components were similar to the C33 to C36 methoxy or keto 1,3-diols isolated previously from M. tuberculosis. Dimycocerosates of phthiocerol A have been described previously; the dimycocerosates of phthiocerol B and phthiodiolone A have, in this study, been isolated for the first time." @default.
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- W2085211212 date "1983-10-01" @default.
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- W2085211212 title "Characterization of phthiocerol dimycocerosates from Mycobacterium tuberculosis" @default.
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