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• W2085232407 abstract "Treatment of a germabenzene (4) bearing a Tbt group (Tbt=2,4,6-tris[bis(trimethylsilyl)methyl]phenyl) with elemental sulfur gave a 1,2,3,4-trithiagermolane (5) together with a novel 1,2,3,4,5,6-pentathiagermepane (6), which is the germanium analog of pentathiepane. On the other hand, the reaction of 4 with elemental selenium gave only 1,2,3,4-triselenagermolane (7). All the newly obtained polychalcogenides containing a germanium atom were characterized by NMR spectroscopy and elemental analysis. The molecular structures of 5 and 6 were determined by X-ray crystallographic analysis. In addition, the thermolyses of 5 and 6 were examined." @default.
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• W2085232407 date "2003-04-01" @default.
• W2085232407 modified "2023-10-16" @default.
• W2085232407 title "Reaction of a stable germabenzene with chalcogens: synthesis and structure of a novel germanium analog of pentathiepane, 1,2,3,4,5,6-pentathiagermepane" @default.
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• W2085232407 doi "https://doi.org/10.1016/s0022-328x(03)00141-4" @default.
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