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- W2085260464 abstract "The crystal structures of the title complexes, Rb[NpO2(NO3)3](1) and Na[NpO2(O2CMe)3](3), have been determined using X-ray diffraction methods. Complex (1) is hexagonal, space group Rc, with hexagonal-bipyramidal co-ordination about the neptunium atom due to three bidentate nitrate groups. Complex (3) is cubic, space group P213, with hexagonal-bipyramidal co-ordination of three bidentate acetate groups to the neptunium atom. The neptunium–ligand oxygen distances in (1) and (3) fall in the range 2.46–2.47 A and in the NpO22+ group are 1.731(18)A in (1) and 1.765(7) and 1.786(7)A in (3). Lattice parameters are: for (1), a= 9.281(2), c= 19.033(4)A, and Z= 6; for (3), a= 10.638(4)A and Z= 4. The structures have been refined to R values of (1) 0.067 and (3) 0.046 using, respectively, 305 and 632 observed diffractometer-measured intensities." @default.
- W2085260464 created "2016-06-24" @default.
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- W2085260464 date "1982-01-01" @default.
- W2085260464 modified "2023-10-07" @default.
- W2085260464 title "Actinide structural studies. Part 2. Crystal and molecular structures of rubidium tris(nitrato)dioxoneptunate(1–) and sodium tris(acetato)dioxoneptunate(1–)" @default.
- W2085260464 doi "https://doi.org/10.1039/dt9820000033" @default.
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