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- W2085263628 abstract "The synthesis of six analogs of N,N′-diacetylchitobiose is reported, including a novel transglycosylation reaction for the preparation of S-aryl thioglycosides. The conformations of the compounds were studied by a combination of NMR spectroscopy and molecular modeling, using force field calculations. In the case of the S-aryl thioglycosides with exclusively S-glycosidic linkages, dihedral angles of the disaccharidic S-glycosidic bonds, Φ′ and Ψ′ and of the S-arylglycoside bonds, Φ and Ψ, were found to be similar, whereas they were different in mixed glycosides and in a thiazoline derivative. An adequate correlation between the calculated H,H-distances of the local minima and the measured NOE contacts was achieved by applying population-weighted averages over participating conformers based on weighted relative energies." @default.
- W2085263628 created "2016-06-24" @default.
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- W2085263628 date "2009-05-01" @default.
- W2085263628 modified "2023-09-26" @default.
- W2085263628 title "Synthesis and conformational analysis of glycomimetic analogs of thiochitobiose" @default.
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- W2085263628 doi "https://doi.org/10.1016/j.tet.2009.03.067" @default.
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