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- W2085282153 abstract "Abstract Summary: Soluble multicyclic polyethers have been prepared by the polycondensation of tetra(bromomethyl)methane with various diphenols. The influence of the diphenol on the competition between cyclization and chain growth (yielding insoluble gels) is studied for feed ratios of 2/1 (a 2 /b 4 monomer) and high conversions. With 4‐ tert ‐butylcatechol or 2,2′‐dihydroxy‐1,1′‐binaphthyl, mainly monomeric spiro‐cycles are formed. Soluble multicycles free of end‐groups are only obtained from α , ω ‐bis(3‐hydroxyphenoxy) alkanes. The structure of the reaction products has been characterized by 1 H NMR spectroscopy and MALDI‐TOF mass spectrometry. As characteristic properties of the compact multicyclic structure, low solution viscosities in combination with high polydispersities are found. DSC measurements prove an amorphous character with glass‐transition temperatures in the range of 45–85 °C. Formation of soluble multicyclic oligoethers. image Formation of soluble multicyclic oligoethers." @default.
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- W2085282153 date "2006-08-29" @default.
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- W2085282153 title "Multicyclic Polyethers Derived from Tetra(bromomethyl)methane and Flexible Diphenols" @default.
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- W2085282153 doi "https://doi.org/10.1002/macp.200600233" @default.
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