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- W2085284466 abstract "Abstract Two three-dimensional open-framework zinc phosphites with the same organically templated, [H 2 pip][Zn 3 (HPO 3 ) 4 (H 2 O) 2 ] ( 1 ) and K[H 2 pip] 0.5 [Zn 3 (HPO 3 ) 4 ] ( 2 ) (pip = piperazine), have been solvothermally synthesized and structurally characterized by IR, elemental analysis, thermogravimetric analysis, powder and single-crystal X-ray diffractions. Compound 1 consists of ZnO 4 tetrahedra, [HPO 3 ] pseudopyramids and [ZnO 4 (H 2 O) 2 ] octahedra, which are linked through their vertexes to generate three-dimensional architecture with intersecting 8-membered channels along the [1 0 0], [0 0 1] and [1 0 1] directions. Compound 2 is constructed from strictly alternating ZnO 4 tetrahedra and [HPO 3 ] pseudopyramids, and exhibits (3,4)-connected inorganic framework with 8-, and 12-membered channels, in which the K + and diprotonated H 2 pip 2+ extra-framework cations reside, respectively. The coexistence of inorganic K + and organic piperazine mixed templates in the structure is unique and, to the best of our knowledge, firstly observed in metal-phosphite materials. In addition, the participation of left-handed and right-handed helical chains in construction of the puckered 4.8 2 sheet structure in 2 is also noteworthy." @default.
- W2085284466 created "2016-06-24" @default.
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- W2085284466 date "2014-01-01" @default.
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- W2085284466 title "Two new three-dimensional zinc phosphites templated by piperazine: [H2pip][Zn3(HPO3)4(H2O)2] and K[H2pip]0.5[Zn3(HPO3)4]" @default.
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- W2085284466 doi "https://doi.org/10.1016/j.molstruc.2013.10.025" @default.
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