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- W2085304867 abstract "Radiation-induced damage to the steroid progesterone has been studied. In the single-crystal form progesterone was exposed to X rays at room temperature and the stable radical thus formed was studied at that temperature. ENDOR observations in four planes of rotation showed that the induced radical is formed by hydrogen abstraction from C6 which leaves unpaired spin density to the O3, C4, C6 region. The hyperfine splitting tensors obtained are ascribed to five specific protons in the molecule (H4 and H6B, H7A, H7B, and H2A). Information on the radical structure is obtained by a correlation of the tensor data with directions in the undamaged molecule. The present data suggest that H6A is removed, whereupon some minor molecular changes take place involving a displacement of C6 of approximately 0.1 Å and H6B of 0.4 Å The remaining part of the molecule seems to be unchanged." @default.
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- W2085304867 date "1985-06-01" @default.
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- W2085304867 title "An ENDOR study of radiation-induced molecular damage to progesterone" @default.
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- W2085304867 doi "https://doi.org/10.1016/0022-2364(85)90324-5" @default.
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