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- W2085384782 abstract "Short transverse relaxation times of Calpha and Cbeta single-quantum coherences reduce the sensitivity of triple-resonance experiments involving transfers of Calpha/Cbeta or Halpha/Hbeta coherences. Multiple-quantum line-narrowing techniques improve the relaxation properties of 13C coherences, thereby increasing the sensitivity of the experiment. In the present work, we describe PFG-CBCA(CO)NH and PFG-HBHA(CO)NH experiments that utilize heteronuclear multiple-quantum coherences in a simultaneous constant-time period to obtain completely decoupled spectra with improved sensitivity. Results indicate that approximately 30% of cross peaks show an average enhancement of approximately 15% in the CBCA(CO)NH experiment. In the related HBHA(CO)NH experiment, approximately 97% of the cross peaks show an average enhancement of approximately 40%." @default.
- W2085384782 created "2016-06-24" @default.
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- W2085384782 date "1999-04-01" @default.
- W2085384782 modified "2023-10-18" @default.
- W2085384782 title "Sensitivity-Enhanced Sim-CT HMQC PFG-HBHA(CO)NH and PFG-CBCA(CO)NH Triple-Resonance Experiments" @default.
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- W2085384782 doi "https://doi.org/10.1006/jmre.1998.1699" @default.
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