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- W2085394310 abstract "Catechol-U-14C and hydroquinone-U-14C were prepared from phenol-U-14C by mononitration followed by chromatographic separation of o- and p-nitrophenol-U-14C. The nitrophenols were separately hydrogenated, and the resulting aminophenols were converted by diazotization followed by hydrolysis to the title diols. Phenol-U-14C was synthesized efficiently from benzene by nitration, reduction, diazotization and hydrolysis. A similar series of reactions beginning with benzene-U-13C gave phenol, catechol and hydroquinone containing more than 88% total carbon-13." @default.
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- W2085394310 date "1981-04-01" @default.
- W2085394310 modified "2023-10-16" @default.
- W2085394310 title "Preparation of uniformly 14C-labeled and 13C-enriched catechol and hydroquinone via phenol" @default.
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- W2085394310 doi "https://doi.org/10.1002/jlcr.2580180410" @default.
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