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• W2085397568 endingPage "2848" @default.
• W2085397568 startingPage "2841" @default.
• W2085397568 abstract "The phase transformation from kaolinite to mullite was examined with new electron diffraction data obtained using an energy-filtering transmission electron microscope. Kaolinite was finally transformed to mullite and cristobalite through several steps of endothermic and exothermic reactions, which resulted in metakaolinite, a microcrystalline spinel-type phase and amorphous silica. Metakaolinite maintained its short-range order even at 920°C. The spinel-type phase resulted from a topotactic transformation of metakaolinite. Mullite first appeared at around 940°C, showing no clear crystallographic relationships to the parent metakaolinite structure. It coexisted with metakaolinite and the spinel-type phase produced previously. The first strong exothermic peak on the DTA curve was mainly due to the extraction of amorphous silica from metakaolinite and the gradual nucleation of the mullite phase. The initially formed spinel-type and mullite phases were suggested to be Al-rich, but to progressively gain Si in their structures at higher temperatures. The spinel-type phase decomposed completely through a second weak exothermic reaction, promoting the crystallization of cristobalite from amorphous silica, and the growth of mullite." @default.
• W2085397568 created "2016-06-24" @default.
• W2085397568 creator A5045914451 @default.
• W2085397568 creator A5077462603 @default.
• W2085397568 creator A5091284091 @default.
• W2085397568 date "2004-12-21" @default.
• W2085397568 modified "2023-09-27" @default.
• W2085397568 title "Phase Transformation Sequence from Kaolinite to Mullite Investigated by an Energy-Filtering Transmission Electron Microscope" @default.
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• W2085397568 doi "https://doi.org/10.1111/j.1151-2916.1999.tb02165.x" @default.
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