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- W2085453203 abstract "Abstract An innovative synthesis of inorganic fullerene-like disulfide tungsten (IF-WS 2 ) nanoparticles was developed using a chemical reduction reaction in a horizontal quartz reactor. In this process, first tungsten trisulfide (WS 3 ) was formed via a chemical reaction of tetra thiotungstate ammonium ((NH 4 ) 2 WS 4 ), polyethylene glycol (PEG), and hydrochloric acid (HCl) at ambient temperature and pressure. Subsequently, WS 3 was reacted with hydrogen (H 2 ) at high temperature (1173–1373 K) in a quartz tube. The produced WS 2 nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray (EDAX), and transmission electron microscopy (TEM). The characterization results indicated that the high-purity (100%) IF-WS 2 nanoparticles were produced. Moreover, addition of surfactant (PEG) and higher operating temperature (1173–1373 K) decreased the particles agglomeration, and consequently led to the reduction of average diameter of WS 2 particles in the range of 50–78 nm. The developed method is simple, environmentally compatible, and cost-effective in contrast to the conventional techniques." @default.
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- W2085453203 date "2010-05-01" @default.
- W2085453203 modified "2023-10-14" @default.
- W2085453203 title "IF-WS2 nanoparticles size design and synthesis via chemical reduction" @default.
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- W2085453203 doi "https://doi.org/10.1016/j.materresbull.2010.01.020" @default.
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