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• W2085479894 abstract "An electrically heated tungsten coil was used as a trap in the determination of antimony. The technique consists of three steps. Initially, SbH3 is formed by hydride generation procedure; then the analyte species in vapor form are transported to W-coil trap heated at 370 °C. Following the preconcentration step, the trap is heated to 895 °C; analyte species are revolatilized and transported to the flame-heated quartz atom cell where atomization and the formation of signal take place. The experimental parameters were optimized both for trap and no-trap studies. The most important experimental parameters are concentrations of HCl and NaBH4 solutions, H2 and Ar gas flow rates, and collection and revolatilization temperatures of W-coil. Accuracy was tested using a certified reference material, waste water EU-L-1. Limit of detection for the system is 16 ng l− 1 using a sample of 36 ml collected in 4.0 min. Enhancement factor in sensitivity was 17." @default.
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• W2085479894 date "2008-08-01" @default.
• W2085479894 modified "2023-10-10" @default.
• W2085479894 title "Determination of antimony by using tungsten trap atomic absorption spectrometry" @default.
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• W2085479894 doi "https://doi.org/10.1016/j.sab.2008.03.021" @default.
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