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- W2085493845 abstract "Deuterated syringolide 2 3 was prepared from D-xylulose and 8-bromooctanoic acid by a convergent route based on our previously reported biomimetic synthesis of this microbial elicitor. Key steps were the thermal acylation of the anisylidene-protected sugar 6 with the C-octenoyl Meldrum's acid derivative 7b, the one-pot triple-cyclisation of the xylulose β-ketoester 9b to 9,10-dehydrosyringolide 2 (10), and the introduction of multiple deuterium labels in the side chain by catalytic exchange and reduction. The route is applicable to the synthesis of tritium labelled syringolide 2 4. © 1998 John Wiley & Sons, Ltd." @default.
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- W2085493845 date "1998-03-01" @default.
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- W2085493845 title "Synthesis of the microbial elicitor syringolide 2 multiply labelled with deuterium" @default.
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- W2085493845 doi "https://doi.org/10.1002/(sici)1099-1344(199803)41:3<211::aid-jlcr69>3.0.co;2-9" @default.
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