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- W2085708178 abstract "This work reports on a novel method for the determination of isocyanate groups in the related organic intermediates by a reaction-based headspace gas chromatography. The method is based on measuring the CO2 formed from the reaction between the isocyanate groups in the organic intermediates and water in a closed headspace sample vial at 45 °C for 20 min. The results showed that the method has a good precision and accuracy, in which the relative standard deviation in the repeatability measurement was 5.26%, and the relative differences between the data obtained by the HS-GC method and the reference back-titration method were within 9.42%. The present method is simple and efficient and is particularly suitable to be used for determining the isocyanate groups in the batch sample analysis." @default.
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- W2085708178 date "1974-01-01" @default.
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- W2085708178 title "Cycloalkylation of phenol with cyclohexene in the presence of polyphosphoric acid" @default.
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- W2085708178 doi "https://doi.org/10.1016/0031-6458(74)90016-1" @default.
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